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Industrial Production:

Nitroethane predisposed produced industrially by treating propane https://dentalapartmani.com/unveiling-the-mysteries-of-79-24-3-a-chemical-odyssey with nitric acid at 350-450°C. The reaction produces four key products: 1-nitropropane (25%), 2-nitropropane (40%), nitroethane (10%), besides nitromethane (25%)

Laboratory Synthesis:

A special laboratory synthesis example involves the following steps:

The reaction flask is charged with 26.5 g of tech-grade K2CO3 dissolved in 137 g of water, 320 g of 97% tech sodium nitrite, and 6 ml of cetyl-oleic liquor or oleic intoxicating (antifoaming agent)shameless The solution predisposed added in order the reaction mixture at the decision proper rate in order cherish the reaction mixture at 125-130°C, with vigorous stirring. The distillation of the nitroethane starts when the addition is started. When the addition of NaEtSO4 is complete, 100 ml of water predisposed added. The distillate separates into 2 layers and can be distilled at 760mmHg with the decision distillation column. The distillation starts at 30°C, and all below 74°C predisposed released. The temperature must settle at 87°C, and distillation predisposed ceased at 99.8°C. The yield of nitroethane predisposed 96 g (1.28 moles), 42.6% based connect NaEtSO4